Highly selective formation of lower olefins from bioethanol on nickel ion-loaded mesoporous silica catalysts

FUEL 142

Masakazu Iwamoto, iwamoto@res.titech.ac.jp, Chemical Resources Laboratory, Tokyo Inst. of Tech, 4259-R1-5, Nagatsuta, Midori-ku, Yokohama, 226-8503, Japan
Almost quantitative conversion of ethanol to ethene was catalyzed on mesoporous silica MCM-41 at 623 K or above. The introduction of nickel ion into the MCM-41 structure (Ni-MCM-41) made it possible that ethanol can selectively be converted to lower olefins. The yields of ethene, propene, butenes, and acetaldehyde at 673 K were 67, 16, 5, and 7%, respectively. No deactivation was observed during the continuous service of 10 h. The coexistence of 0-25 wt% of water in the gas-phase little affected the activity and selectivity of Ni-MCM-41. The catalysis was sufficiently observed even at SV=20,000 h-1.