CHED 423 |
| The synthesis of (2,6-dimethylphenyl)-triphenylmethane (I) produces several products. (Powers, Boeltz, and Drahl – 231st ACS National Meeting, 2006; Strohl and Powers 233rd ACS Meeting 2007) Improved synthesis of compound V was accomplished along with purification to 99.5%, mp. 79.0 – 81.5. Separation of the byproducts of the reaction of compound V with aniline hydrochloride was accomplished by ether/water extraction at controlled pH's and by column chromatography. The fixed phase was silica gel and the mobile phase was a combination of diethyl ether and ethanol. The GC/MS results for the various compounds will be reported. |
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Undergraduate Research Poster Session: Organic Chemistry
11:00 AM-1:00 PM, Monday, April 7, 2008 Morial Convention Center -- Hall A, Poster
Division of Chemical Education |