FUEL 234 |
| Single-walled carbon nanotubes (SWNTs) "super-powers" include the following: they are ~50 times stronger than steel, have ~1000 times the electron density of copper, and withstand 5072*F in a vacuum. These "super-powers" can be utilized for energy applications such as solar cells, super capacitors, hydrogen storage, and electrochemical devices. We converted pristine SWNTs to 4-chlorophenyl-SWNTs 1 via treatment with 4-chlorophenylamine and isoamylnitrite. Subsequently, we converted 1 to 4-mercaptophenyl-SWNTs by using ethyl thiolate 2. Products 1 and 2 were characterized by Raman, UV-Vis, IR, TGA, and 1H NMR. Our COSY, ROSEY, and NOESY 1H NMR of 1 are the first such spectra reported for a covalently sidewall-functionalized SWNT suspended in solution. We will reveal the results of our NMR studies of several functionalized SWNTs and their "super-powers". |
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Chemistry of Carbon Materials and Nanomaterials
8:30 AM-11:45 AM, Thursday, April 10, 2008 Morial Convention Center -- Rm. 240/241, Oral
Sci-Mix
Division of Fuel Chemistry |