Novel synthesis of poly(tert-butyl acrylate-block-vinyl acetate) copolymers

POLY 83

Christy D. Petruczok, petruccd@clarkson.edu, Richard F. Barlow, barlowrf@clarkson.edu, and Devon A. Shipp, dshipp@clarkson.edu. Department of Chemistry and Biomolecular Science, Clarkson University, Potsdam, NY 13699-5810
Low polydispersity poly(tert-butyl acrylate) has been synthesized using atom transfer radical polymerization. The bromine atoms at the end of the polymer chains were replaced by xanthate moieties; the presence of the xanthate groups was confirmed by 1H NMR spectroscopy and the appearance of a peak at 357 nm in the tert-butyl acrylate UV-visible spectrum. Subsequent reversible addition-fragmentation chain transfer polymerization of the altered poly(tert-butyl acrylate) yielded poly(tert-butyl acrylate-block-vinyl acetate). Molecular weight measurements and 1H NMR spectra confirmed block copolymer formation.
 

Undergraduate Research in Polymer Science
1:30 PM-4:50 PM, Sunday, April 6, 2008 Hilton New Orleans Riverside -- Grand Salon 16, Oral

Division of Polymer Chemistry

The 235th ACS National Meeting, New Orleans, LA, April 6-10, 2008