High molecular weight conjugated polymer nanoparticles from step-growth coupling

POLY 82

Moritz Baier, Johannes Huber, and Stefan Mecking, stefan.mecking@uni-konstanz.de. Department of Chemistry, University of Konstanz, Universitaetsstr. 10, 78464 Konstanz, Germany
High-molecular-weight conjugated polymer nanoparticles with average particle sizes of around 30 nm and molecular weights of up to Mn = 4.1 x 104 g mol-1 have been prepared for the first time in aqueous emulsion. For this step growth polymerization the Glaser coupling was used as a high yield reaction. A key to conducting such reactions in aqueous emulsion was found to be the utilization of the lipophilic bidentate ligand dinonylbipyridine in the copper(I/II) catalyst employed. A copolymerizable diethynyl substituted perylenediimide derivative was synthesized and incorporated covalently into the conjugated polymers. An effective energy transfer to incorporated dye occurs in the poly(aryl diethynyl) nanoparticles prepared.
 

Undergraduate Research in Polymer Science
1:30 PM-4:50 PM, Sunday, April 6, 2008 Hilton New Orleans Riverside -- Grand Salon 16, Oral

Division of Polymer Chemistry

The 235th ACS National Meeting, New Orleans, LA, April 6-10, 2008