Doped semicoductor nanoparticle materials for solar hydrogen conversion

CATL 28

Daniel Raftery, raftery@purdue.edu, Enrique Reyes, Karla Reyes, Yanping Sun, and Guangtao Li. Department of Chemistry, Purdue University, 560 Oval Drive, West Lafayette, IN 47907
Solar-driven water splitting represents an almost ideal and potentially enormous source of energy. Pioneering work was performed many years ago, however, a number of challenges limit the efficiency and applicability of this technology. Most materials that are capable of water-splitting are either limited in their activity to the UV region, where there is little solar energy, or are not sufficiently stable for long term use. A new approach in the field is the use of main group elements for anion-doping of TiO2 and other metal oxides. This approach has shown much improved potential for generating hydrogen efficiently. We have prepared a number of anion-doped metal oxide nanoparticle materials, and several of these show promise for efficient visible photocatalysis, or water-splitting. NMR and other analytical methods are very useful to characterize the detailed chemistry, identify the nature of the dopants, follow the synthetic steps, and relate structure to activity.