Novel phases for normal phase chiral HPLC

ANYL 205

Liya Liu, lliu@ensnano.com, James Zhang, Jeffrey Needham, and Regina Valluzzi, rvalluzzi@ensnano.com. R&D, ENS, 675 Massachusetts Avenue, Cambridge, MA 02139
Chiral analyses for a special branch of analytical chemistry. While there are a number of very general approaches to non-chiral HPLC, chiral HPLC relies on a large number of stationary phases, each with a narrower range of (often unpredictable) chiral selectivity. A new chiral material has been developed with a novel mechanism for chiral selectivity, believed to be more like a chiral exclusion than a chiral analyte-chiral ligand interaction. This mechanism allows chiral selectivity to be decoupled from other chromatographic properties of the stationary phase. A number of non-chiral surface chemical treatments have been performed on this material to determine whether a chiral stationary phase can be developed with good selectivity across a broad range of molecules and good normal phase chromatographic characteristics. Several chemistries will be compared and chromatographic data presented for ionizable pharmaceutical molecules.
 

General Posters
7:00 PM-9:00 PM, Sunday, August 19, 2007 BCEC -- Exhibit Hall - B2, Poster

Sci-Mix
8:00 PM-10:00 PM, Monday, August 20, 2007 BCEC -- Exhibit Hall - B2, Sci-Mix

Division of Analytical Chemistry

The 234th ACS National Meeting, Boston, MA, August 19-23, 2007