Organo-catalyzed ring-opening polymerization of o-carboxyanhydrides

POLY 258

Didier Bourissou, dbouriss@chimie.ups-tlse.fr, Laboratoire Hétérochimie Fondamentale et Appliquée, Université Paul Sabatier, 118 Route de Narbonne, 31062 Toulouse Cedex 4, France
Lactide is a moderately polymerizable monomer, so that highly active promoters are required to mediate its ROP under mild conditions. The O-carboxyanhydride derived from lactic acid (lacOCA) was found to be a promising synthetic equivalent of lactide, exhibiting remarkable reactivity in nucleophile-catalyzed ROP. Accordingly, PLAs of controlled molecular weights and narrow polydispersities are typically obtained under mild conditions using DMAP and various protic initiators. The preparation of variously substituted poly(alpha-hydroxyacids) will also be discussed, as well as the enzymatic polymerization of lacOCA using lipases.
 

Polymers from Renewable Resources
8:20 AM-11:45 AM, Monday, August 20, 2007 Westin Boston Waterfront -- Douglas, Oral

Division of Polymer Chemistry

The 234th ACS National Meeting, Boston, MA, August 19-23, 2007