Platform chemicals from cellulose, saltwater and microwaves

I&EC 14

J. Michael Robinson, robinson_m@utpb.edu, Anna Arce, Staci Barrett, Tamara Byrd, Robert Caudle, Steven Davila, Joseph Phillips, Elizabeth Salinas, and Drew Worth. Department of Chemistry, University of Texas of the Permian Basin, 4901 East University Blvd., Odessa, TX 79762
α-Crystalline cellulose is the most recalcitrant portion of biomass carbohydrates. Under the usually severe and acidic conditions required for digestion of this fraction, most of the desired aldose platform chemical (glucose) reacts further to undesired mixtures. However, replacing the usual Bronsted acid catalyst with certain salts, which are sensitive to microwave heating, enhances the relative rate of cellulose dissolutions and allows some selectivity of product. Thus, various salt-microwave methods afford good conversions of α-crystalline cellulose to certain platform chemicals. Separation and recycle of the saltwater may assist the economics of such processes.