A sensitive immunoassay for the detection of spinosyns in industrial water

AGRO 49

Guomin Shan, gshan@dow.com1, Thomas Sparks1, Gary D. Crouse, gdcrouse@dowagro.com1, Michael Abraham1, Carol Fess1, Titan S. Fan, brians@beaconkits.com2, and Brian A. Skoczenski2. (1) Regulatory Laboratories, Dow AgroSciences LLC, 9330 Zionsville Rd, Indianapolis, IN 46268, (2) Beacon Analytical Systems, 383 Presumpscot Street, Portland, ME 04103
The spinosyns belong to a new family of insect control agents that are derived from a naturally occurring soil bacterium Saccharopolyspora spinosa. Spinosad, which comprises spinosyns A and D, is widely used on a variety of crops to control several orders of insects. Spinetoram, which contains derivatives of both spinosyns J and L, is being developed at Dow AgroSciences and is expected to be introduced to the market soon. A rapid and sensitive immunoassay for detecting all active ingredients of spinosad and spinetoram was developed. Rabbits were immunized with 5,6-dihydro spinosyn A, 3'-O-glutarate-thyroglobulin conjugate. All sera were screened against numerous HRP conjugated antigens. The assay with the least interference and the best sensitivity was optimized and characterized. The average I50 for spinosyn A was 0.09 ppb with a detection limit of 0.02 ppb. The resulting assay equally detects all four active ingredients of both spinosyn and spinetoram. No or minimal cross reactivity was found to other spinosyn metabolites. The assay was validated for industrial waste water monitoring. Results of validation and application in waste water matrix will be discussed.
 

New Developments and Issues in Agrochemical Sciences
8:00 AM-11:00 AM, Monday, August 20, 2007 BCEC -- Exhibit Hall - B2, Poster

Sci-Mix
8:00 PM-10:00 PM, Monday, August 20, 2007 BCEC -- Exhibit Hall - B2, Sci-Mix

Division of Agrochemicals

The 234th ACS National Meeting, Boston, MA, August 19-23, 2007