A novel template for the formation of water-soluble conducting polymers

POLY 437

Ferdinando Bruno, Ferdinando_Bruno@uml.edu1, Subhalakshmi Nagarajan, mailtosubha@yahoo.com2, Ramaswamy Nagarajan, ram@uml.edu2, Jayant Kumar, Jayant_Kumar@uml.edu3, and Lynne A. Samuelson, Lynne_Samuelson@uml.edu4. (1) U.S Army Natick Soldier Center, RDECOM, Kansas street, Natick, MA 01760, (2) Department of Chemistry, Center for Advanced Materials, University of Massachusetts, Lowell, One University Avenue, Lowell, MA 01854, (3) Departments of Physics, Center for Advanced Materials, University of Massachusetts Lowell, Lowell, MA 01854, Lowell, MA 01854, (4) U.S. Army RDECOM, Natick Soldier Center, Kansas Street, Natick, MA 01760
Enzymatic and synthetic enzymatic template-assisted polymerization of phenol and aniline has been carried out in water at room temperature. Various bio-compatible polymers such as Chondroitin sulphate (CHO), Kerathan sulphate (KER), and Dermatan (sulphate (DER) have been used as templates. These templates help in orienting the momomers (phenols and anilines) prior to and during the polymerization. Horseradish peroxidase proved to be an effective catalyst for this polymerization. In addition alternative synthetic enzyme, pegylated Iron Porphyrin (PEG-Hematin), was also found to catalyze the polymerization yielding more stable and cost effective polymeric complexes with electrical and antioxidant properties. All the products were soluble in water. UV-Vis spectroscopy indicated the presence of a large backbone conjugation. Furthermore, a naturally occurring phenolic compound, (-) epicatechin (NEP), was also polymerized in presence of CHO, KER and DER. The product exhibited higher stability, compared to the monomer, opening new avenues for application in the areas of food and medicine. This novel synthetic approach leads to improved processability, and functional characteristics for the polymer.