Ultrafast relaxation dynamics of the “ammoniated” electron from liquid metal-ammonia solution

PHYS 26

Jörg Lindner1, Andreas N. Unterreiner, andreas.unterreiner@chemie.uni-karlsruhe.de2, and Peter Vöhringer, p.voehringer@uni-bonn.de1. (1) Department of Chemistry, University of Bonn, Institute for Physical Chemistry, Wegelerstrasse 12, Bonn, 53115, Germany, (2) Institute of Physical Chemistry, University of Karlsruhe, Kaiserstr. 12, Karlsruhe, 76128, Germany
We have performed the first femtosecond near-infrared pump-probe experiments of equilibrated solvated electrons from liquid metal-ammonia solutions. The studies were carried out at electron concentrations of (2±1)E-4 mol/l corresponding to dilute solutions dominated by paramagnetic electrons with negligible spin-pairing. Using excitation pulses centered at 1280 nm, the dynamics were recorded for probe wavelengths ranging from 1200 and 2100 nm with a time resolution of roughly 100 fs. Immediately after photoexcitation, the absorption spectrum of the solvated electrons is strongly red-shifted with respect to their steady-state spectrum. Subsequently, a dynamic spectral blue-shift is observed that occurs with a time constant of (150±50) fs. A thorough analysis based on a dynamically evolving Kubo line-shape with a minimal number of fitting parameters demonstrates that these experiments can be understood either in terms of a simple temperature-jump model or in terms of a local density jump scenario. Non-adiabatic relaxation dynamics from the initially accessed “p-like” excited sate back to the “s-like” ground electronic state occur on a time scale faster than 100 fs. The results are compared with complementary experiments on the hydrated electron in aqueous bulk phases or on size-selected negative ion clusters.