Improved traceability of chemical agent standard analytical reference material (CASARM)

ANYL 58

Howard Elbaum, Edgewood Chemical Biological Center, 5183 Blackhawk Road, Attn: AMSSR-ECB-CB-SC, Aberdeen Proving Ground, MD 21010 and Gary Kramer, Analytical Chemistry Division, National Institute of Standards and Technology, Chemical Science and Technolgy Laboratory, Building 227, Room A-163, Gaithersburg, MD 20899-8394.
The Chemical Agent Standard Analytical Reference Material (CASARM) Program was established by the U.S. Army in 1986 to provide and maintain high quality, well characterized chemical agent standards. These CASARMs are used by U.S. chemical agent storage and demilitarization organizations, research laboratories, installation restoration activities and contractors. The Central Quality Assurance Laboratory at the Edgewood Chemical Biological Center uses several different methods such as NMR, titration and gas chromatography for determination of purity and identification of impurities in neat materials. Traceability of the reference materials to a national standard is achieved for most of the materials in the repository through titration methods with limited specificity. An effort to improve specificity is underway through the development of organo-phosphorus reference materials to be used in conjuction with quantitative NMR methods. The background of the CASARM program and progress to certify organophosphorus reference materials will be presented.
 

General Papers
7:00 PM-9:00 PM, Sunday, 10 September 2006 Moscone Center -- Hall D, Poster

Division of Analytical Chemistry

The 232nd ACS National Meeting, San Francisco, CA, September 10-14, 2006