Synergistic effects of pH, ionic strength and enzyme concentration on stimuli-responsive behavior of colloidal films

POLY 431

Min Yu, marek.urban@usm.edu and Marek W. Urban, marek.urban@usm.edu. School of Polymers and High Performance Materials, The University of Southern Mississippi, Department of Polymer Science, 118 College Drive, PO 10076, Hattiesburg, MS 39406
Previous studies showed methyl methacrylate (MMA) and n-butyl acrylate (nBA) were polymerized to form stable colloidal particles in the presence of sodium dioctyl sulfosuccinate (SDOSS) and 1,2-dilauroyl-sn-glycero-3-phosphocholine (DLPC) in aqueous phase. Stimuli-responsive behaviors of these colloidal dispersions were investigated and various stimuli drive molecular entities to designated areas of coalesced films. In this study, we focus on the synergistic stimuli-responsive characteristics of the phospholipid stabilized colloidal dispersions such as the combined effects of ionic strength, enzyme, and pH on the mobility of dispersion stabilizing agents within p-MMA/nBA copolymer matrixes during and after coalescence. Attenuated total reflectance Fourier transform infrared (ATR FT-IR) spectroscopy of p-MMA/nBA colloidal dispersions revealed the formation and the preferential orientation of surface localized ionic clusters (SLICs) at the film-air (F-A) or film-substrate (F-S) interfaces in response to the combined stimulus effects. Using this approach it is possible to control surface morphologies of coalesced films.
 

7th International Biorelated Polymers Symposium
6:00 PM-8:00 PM, Tuesday, 12 September 2006 Moscone Center -- Hall D, Poster

Sci-Mix
8:00 PM-10:00 PM, Monday, 11 September 2006 Moscone Center -- Hall D, Sci-Mix

Division of Polymer Chemistry

The 232nd ACS National Meeting, San Francisco, CA, September 10-14, 2006