Low temperature ignition behavior of methyl decanoate

FUEL 12

James Szybist, jps182@psu.edu and Andre L. Boehman, boehman@ems.psu.edu. The Energy Institute, The Pennsylvania State University, 405 Academic Activities Building, University Park, PA 16802
The low temperature ignition behavior of methyl decanoate, a biodiesel relevant compound, was investigated in a motored engine experiment. Premixed charges of fuel and air were delivered to the engine, and the extent of autoignition was controlled by varying the compression ratio. Methyl deaconate exhibited two-stage ignition, with low temperature heat release (LTHR), or cool flame, followed by the main combustion event. FTIR analysis of the exhaust gas revealed that the ester group undergoes decarboxylation, or formation of carbon dioxide through unimolecular decomposition, not oxidation. When decarboxylation occurs in oxygenated diesel fuels, it reduces their effectiveness at reducing PM emissions because the oxygen is not fully utilized. The condensable species produced during LTHR were further analyzed via GC/MS, and a large number of species containing both methyl ester groups and additional carbonyl functionalities were identified. It was concluded the initial LTHR reactions involve only the aliphatic chain and are similar to those of n-heptane. Decarboxylation does not occur until the aliphatic chain has been largely consumed by LTHR reactions.
 

Biofuels for Transportation
8:55 AM-12:05 PM, Sunday, 26 March 2006 Georgia World Congress Center -- C204, Oral

Division of Fuel Chemistry

The 231st ACS National Meeting, Atlanta, GA, March 26-30, 2006